Microwave-assisted extraction of phenolics from Canarium album L. and identification of the main phenolic compound.
Microwave-assisted extraction (MAE) was applied in the extraction of phenolics from Canarium album L. Effects of various conditions including the solvent, solvent to material ratio, microwave power and irradiation time on extraction yield of phenolics were investigated. In terms of the optimal conditions of MAE, it was concluded that 70% (v/v) of ethanol was the proper extraction solvent, the solvent to material ratio was 10 : 1 (mL : g), and the microwave power and irradiation time were 600 W and 15 s, respectively. Compared with normal stirring extraction and ultrasound-assisted extraction, the MAE of phenolics from C. album L. was more time efficient and gave a high extraction rate. More than 1.2% extraction yield was achieved with MAE, and the purity of the phenolics in the extract product was up to 25%. In addition, by ultraviolet-visible (UV) spectrometry and electrospray ionised mass spectrometry (ESI/MS), the main phenolic compound in the extract product was identified as gallic acid.
State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi, Jiangsu 214122, China. hzy9501@yahoo.com.cn
Zhiyong
Z
He
Wenshui
W
Xia
D029403:Burseraceae / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid; D008872:Microwaves; D010636:Phenols / Q000302:isolation & purification*; D021241:Spectrometry, Mass, Electrospray Ionization; D013056:Spectrophotometry, Ultraviolet
D010636:Phenols