title: [Determination of chloramphenicol residues in milk powder using molecular imprinted polymers (MIP) by LC-MS/MS].
abstract: The method is presented to analyze chloramphenicol in milk powder. Sample was clean-up by used molecular imprinted polymers (MIP). The determination was performed by LC-ESI-MS/MS. The LC was equipped with column Luna C18 Phenomenex. CAP-d5 was used as internal standards. The method was validation according to the criteria of Decision Commission No 2002/657/EC. Recoveries for the level 0.3 microg/kg was in the range 104-111%. The limit of decision (CCalpha) and detection capability (CCbeta) was respectively 0.06 microg/kg and 0.09 microg/kg.
authors.affiliation: Zakad Higieny Weterynaryjnej, Wojewódzki Inspektorat Weterynarii, Białystok. rodziewicz@wiw.bianet.com.pl
authors.forename: Lech
authors.initials: L
authors.lastname: Rodziewicz
authors.forename: Iwona
authors.initials: I
authors.lastname: Zawadzka
mesh_terms: D000818:Animals; D000900:Anti-Bacterial Agents / Q000032:analysis*; D002701:Chloramphenicol / Q000032:analysis*; D002849:Chromatography, Gas / Q000379:methods; D002853:Chromatography, Liquid; D005506:Food Contamination / Q000032:analysis*; D006801:Humans; D008892:Milk / Q000737:chemistry*; D054802:Molecular Imprinting / Q000379:methods; D011044:Poland
chemical_list: D000900:Anti-Bacterial Agents; D002701:Chloramphenicol