title: 3-Bromo-N'-(3,5-dibromo-2-hydroxy-benzyl-idene)benzohydrazide methanol solvate.
abstract: The title compound, C(14)H(9)Br(3)N(2)O(2)·CH(4)O, was prepared by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde and 3-bromo-benzohydrazide in methanol. The asymmetric unit of the crystal consists of a Schiff base mol-ecule and a methanol mol-ecule of crystallization. The dihedral angle between the two benzene rings is 5.5 (2)°. An intra-molecular O-H⋯N hydrogen bond is observed. In the crystal structure, pairs of adjacent Schiff base mol-ecules are linked by two methanol mol-ecules through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.
authors.affiliation: Department of Chemistry, Huainan Normal College, Huainan 232001, People's Republic of China.
authors.forename: Yi-Jun
authors.initials: YJ
authors.lastname: Wei
authors.forename: Feng-Wu
authors.initials: FW
authors.lastname: Wang
authors.forename: Qi-Yong
authors.initials: QY
authors.lastname: Zhu