title: 1-(4-Meth-oxy-benzyl-idene)-4-methyl-thiosemicarbazide.
abstract: The title compound, C(10)H(13)N(3)OS, was prepared by the reaction of 4-meth-oxy-benzaldehyde and 4-methyl-thio-semicarbazide. The dihedral angle between the benzene ring and the thio-urea unit is 8.64 (7)° and an intra-molecular N-H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds generate R(2) (2)(8) loops. The dimers are linked into (001) sheets by further N-H⋯S links.
authors: Microscale Science Institute, Department of Chemistry and Chemical Engineering, Weifang University, Weifang 261061, People's Republic of China.
authors: Yu-Feng
authors: YF
authors: Li
references: Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22
references: 18156677
references: Acta Crystallogr Sect E Struct Rep Online. 2010 May 22;66(Pt 6):o1399
references: 21579478