title: 5-[(E)-Benzyl-idene]-2-hy-droxy-10-methyl-8-phenyl-3,10-diazahexa-cyclo-[10.7.1.1.0.0.0]henicosa-1(19),12(20),13,15,17-pentaen-6-one ethanol 0.25-solvate 0.6-hydrate.
abstract: In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the two phenyl rings is 70.83 (16)°. One of the N atoms of the organic mol-ecule is disordered over two positions in a 0.52 (4):0.48 (4) ratio and the two solvent mol-ecules are partially occupied and show high displacement parameters. In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.
authors: Raju Suresh
authors: RS
authors: Kumar
authors: Hasnah
authors: H
authors: Osman
authors: Subbu
authors: S
authors: Perumal
authors: Madhukar
authors: M
authors: Hemamalini
authors: Hoong-Kun
authors: HK
authors: Fun
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references: 18722036
references: Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55
references: 19171970