title: Spectroscopic and structural properties of N-(acetamide) morpholinium bromide.
abstract: A new crystal of N-(acetamide) morpholinium (NAM) bromide has been prepared in methanol at room temperature and characterized by single crystal X-ray analysis, elemental analysis, GS-MS, FTIR, NMR((1)H,(13)C, DEPTH and HETCOR). The N-(acetamide) morpholinium crystallizes in the orthorhombic crystal system, Pnma with unit cell a=12.798(9) Å, b=7.222(5) Å, c=9.244(5) Å, β=90.00, V=854.4(9) Å(3), Z=4. The X-ray structure determination revealed that there are strong inner and intermolecular hydrogen bonds in the crystal.
authors: Onsekiz Mart University, Art and Science Faculty, Department of Chemistry, 17100 Canakkale, Turkey. yakupbaran@yahoo.com
authors: Yakup
authors: Y
authors: Baran
authors: Hava
authors: H
authors: Ozay
authors: Hasan
authors: H
authors: Esener
authors: Murat
authors: M
authors: Turkyilmaz
mesh_terms: D000081:Acetamides / Q000737:chemistry*; D001965:Bromides / Q000737:chemistry*; D018360:Crystallography, X-Ray; D009682:Magnetic Resonance Spectroscopy; D008954:Models, Biological; D008958:Models, Molecular; D008968:Molecular Conformation; D015394:Molecular Structure; D009025:Morpholines / Q000737:chemistry*; D017550:Spectroscopy, Fourier Transform Infrared; D013057:Spectrum Analysis / Q000379:methods
chemical_list: D000081:Acetamides; D001965:Bromides; D009025:Morpholines