title: Effect of dentin pretreatment with potassium oxalate: analysis of microtensile bond strengths and morphologic aspects.
abstract: An effective and stable bond is the most desirable characteristic of contemporary adhesive systems. The aim of this study was to evaluate the effect of potassium oxalate on dentin/resin bond strength. Dentin on the occlusal surface of human premolars was exposed and etched with 35% phosphoric acid, to receive 3% monohydrated potassium oxalate and the following adhesive systems: Scotchbond Multipurpose (SMO; 3M/ESPE) and Prime & Bond NT (PBO; Dentsply), followed by the application of resin composite (Z250; 3M/ESPE). The control groups (SM and PB) did not receive potassium oxalate application. The prepared teeth were kept in distilled water at 37°C for 24 h and 12 months. They were then cut longitudinally into sticks with a bond area of ∼0.8 mm(2) for submission to the microtensile bond strength test. The data were analyzed by two-factor ANOVA, Tamhane's paired comparisons, and the Student t-test (α = 0.05). The hybrid layer formed was observed by scanning electron microscopy (SEM). SEM analysis of the surfaces treated with PB revealed shorter resin tags associated with the application of potassium oxalate, whereas SM showed tags similar to those without potassium oxalate. A significant difference was shown between the two storage times for each of the protocols. There was a significant difference among SMO, SM, and PBO (24 h), as well as among SM, SMO, and PBO, and between PB and PBO (12 months). The application of potassium oxalate before conventional adhesive systems may result in alteration of the bond strength between dentin and resin composite, depending on the material.
authors.affiliation: Faculdade de Ciências Biológicas e da Saúde, Centro Universitário Cesmac, Maceió (AL), Brazil. isabelcmporto@gmail.com
authors.forename: Isabel Cristina Celerino
authors.initials: IC
authors.lastname: De Moraes Porto
authors.forename: Ana Karina Maciel
authors.initials: AK
authors.lastname: De Andrade
authors.forename: Luiz Carlos
authors.initials: LC
authors.lastname: Alves
authors.forename: Rodivan
authors.initials: R
authors.lastname: Braz
mesh_terms: D000704:Analysis of Variance; D001641:Bicuspid / Q000737:chemistry / Q000187:drug effects / Q000648:ultrastructure; D003188:Composite Resins / Q000494:pharmacology; D001840:Dental Bonding; D003804:Dentin / Q000737:chemistry / Q000187:drug effects*; D017220:Dentin-Bonding Agents / Q000737:chemistry / Q000494:pharmacology; D006801:Humans; D008855:Microscopy, Electron, Scanning; D010070:Oxalates / Q000737:chemistry / Q000494:pharmacology*; D010756:Phosphoric Acids / Q000737:chemistry / Q000494:pharmacology; D025341:Principal Component Analysis; D019279:Resin Cements / Q000737:chemistry; D013696:Temperature; D013718:Tensile Strength; D013997:Time Factors; D014867:Water / Q000737:chemistry
chemical_list: D003188:Composite Resins; D017220:Dentin-Bonding Agents; D010070:Oxalates; D010756:Phosphoric Acids; D019279:Resin Cements; D014867:Water; C041330:Scotchbond; C030242:phosphoric acid