title: In-depth polymerization of a self-adhesive dual-cured resin cement.
abstract: The aim of this study was to assess Knoop hardness at different depths of a dual-cured self-adhesive resin cement through different thicknesses of Empress Esthetic® ceramic.Flattened bovine dentin was embedded in resin. The cement was inserted into a rubber mold (0.8 x 5 mm) that was placed between two polyvinyl chloride plastic films and placed over the flat dentin and light cured by Elipar Trilight-QTH (800 mW/cm2) or Ultra-Lumelight-emitting diode (LED 5; 1585 mW/cm2) over ceramic disks 1.4 or 2 mm thick. The specimens(n=6) were stored for 24 hours before Knoop hardness (KHN) was measured. The data were submitted to analysis of variance in a factorial split-plot design and Tukey's test (a=0.05).There was significant interaction among the study factors. In the groups cured by the QTHunit, an increase in ceramic thickness resulted in reduced cement hardness values at all depths, with the highest values always being found in the center (1.4 mm, 58.1; 2 mm, 50.1)and the lowest values at the bottom (1.4 mm,23.8; 2 mm, 20.2). When using the LED unit, the hardness values diminished with increased ceramic thickness only on the top (1.4 mm,51.5; 2 mm, 42.3). In the group with the 1.4-mm-thick disk, the LED curing unit resulted in similar values on the top (51.5) and center(51.9) and lower values on the bottom (24.2).However, when the cement was light cured through the 2-mm disk, the highest hardness value was obtained in the center (51.8), followed by the top (42.3) and bottom (19.9),results similar to those obtained with the QTH curing unit (center > top > bottom). The hardness values of the studied cement at different depths were dependent on the ceramic thickness but not on the light curing units used.
authors.affiliation: Piracicaba Dental School, Sao Paulo, Brazil. rmpuppin@fop.unicamp.br
authors.forename: R M
authors.initials: RM
authors.lastname: Puppin-Rontani
authors.forename: R G
authors.initials: RG
authors.lastname: Dinelli
authors.forename: A B
authors.initials: AB
authors.lastname: de Paula
authors.forename: S B P
authors.initials: SB
authors.lastname: Fucio
authors.forename: G M B
authors.initials: GM
authors.lastname: Ambrosano
authors.forename: F M
authors.initials: FM
authors.lastname: Pascon
mesh_terms: D000538:Aluminum Silicates / Q000737:chemistry; D000818:Animals; D002417:Cattle; D055117:Curing Lights, Dental / Q000145:classification; D003776:Dental Porcelain / Q000737:chemistry; D003804:Dentin / Q000648:ultrastructure; D017220:Dentin-Bonding Agents / Q000737:chemistry; D006244:Hardness; D055115:Light-Curing of Dental Adhesives / Q000379:methods; D008422:Materials Testing; D010969:Plastics / Q000737:chemistry; D058105:Polymerization; D011143:Polyvinyl Chloride / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry*; D013499:Surface Properties; D013696:Temperature; D013997:Time Factors
chemical_list: D000538:Aluminum Silicates; D017220:Dentin-Bonding Agents; C075815:IPS-Empress ceramic; D010969:Plastics; C483701:Rely X Unicem; D019279:Resin Cements; D003776:Dental Porcelain; D011143:Polyvinyl Chloride