Dual acquisition magic-angle spinning solid-state NMR-spectroscopy: simultaneous acquisition of multidimensional spectra of biomacromolecules.
Fast data collection: a general method for dual data acquisition of multidimensional magic-angle spinning solid-state NMR experiments is presented. The method uses a simultaneous Hartmann-Hahn cross-polarization from (1)H to (13)C and (15)N nuclei and exploits the long-living (15)N polarization for parallel acquisition of two multidimensional experiments.
Department of Chemistry, Minneapolis, MN 55455, USA.
T
T
Gopinath
Gianluigi
G
Veglia
D002247:Carbon Isotopes / Q000737:chemistry; D006859:Hydrogen / Q000737:chemistry; D046911:Macromolecular Substances / Q000737:chemistry*; D009587:Nitrogen Isotopes / Q000737:chemistry; D019906:Nuclear Magnetic Resonance, Biomolecular; D025801:Ubiquitin / Q000737:chemistry
D002247:Carbon Isotopes; D046911:Macromolecular Substances; D009587:Nitrogen Isotopes; D025801:Ubiquitin; D006859:Hydrogen