title: A convenient synthesis and a NMR study of the diammoniate of diborane.
abstract: DADB synthesis: The diammoniate of diborane (DADB) was synthesized in a new metathesis reaction between the diammoniate of monochloroborane and potassium borohydride in liquid ammonia. (1)H and (11)B NMR spectra of DADB are reported. The stability in THF was examined by variable-temperature (11)B NMR spectroscopy.
authors.affiliation: Department of Chemistry, The Ohio State University, Columbus OH 43210, USA.
authors.forename: Hima K
authors.initials: HK
authors.lastname: Lingam
authors.forename: Xuenian
authors.initials: X
authors.lastname: Chen
authors.forename: Ji-Cheng
authors.initials: JC
authors.lastname: Zhao
authors.forename: Sheldon G
authors.initials: SG
authors.lastname: Shore