title: Synthesis and NMR spectral studies of the 7-C₆₀-adduct of n,n-(tetrachlorophthaloyl) dehydroabietylamine.
abstract: The 7-C₆₀-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The ¹H-NMR and ¹³C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C₁ symmetric structure with 6,6-junction of compound was determined.
authors.affiliation: College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China. zhou86zhi@163.com
authors.forename: Zhi
authors.initials: Z
authors.lastname: Zhou
authors.forename: Zhongxiang
authors.initials: Z
authors.lastname: Lin
mesh_terms: D002244:Carbon / Q000737:chemistry; D002247:Carbon Isotopes; D004224:Diterpenes / Q000032:analysis / Q000138:chemical synthesis / Q000737:chemistry*; D019906:Nuclear Magnetic Resonance, Biomolecular; D010795:Phthalic Acids / Q000032:analysis / Q000138:chemical synthesis / Q000737:chemistry*
chemical_list: C573595:7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine; D002247:Carbon Isotopes; D004224:Diterpenes; D010795:Phthalic Acids; D002244:Carbon