title: Influence of preliminary etching on the stability of bonds created by one-step self-etch bonding systems.
abstract: We evaluated the effects of preliminary etching of dentine on the stability of the bond created by one-step self-etch adhesives under different storage conditions. Adper Easy Bond (3M ESPE) and iBond Self-Etch (iBond SE; Heraeus Kulzer) were applied with an etch-and-rinse (i.e. after preliminary phosphoric acid etching for 15 s) or a self-etch approach. Resin-dentine bonded specimens were sectioned perpendicularly to the adhesive interface according to the 'non-trimming technique'. Beams were stored in artificial saliva for 24 h, 6 months, or 1 yr at 37°C, or in 10% NaOCl for 5 h at room temperature, and then stressed until failure; the microtensile bond strengths were calculated. Interfacial nanoleakage of additional teeth was evaluated using light microscopy or transmission electron microscopy. Adper Easy Bond showed higher bond strength than iBond SE, regardless of the dentine treatment. Similar microtensile bond strength results were obtained for teeth subjected to artificial ageing in 10% NaOCl for 5 h at room temperature and for teeth stored in artificial saliva for 6 months at 37°C. The additional etching step increased the microtensile bond strength for Adper Easy Bond and iBond SE. This study supports the use of one-step adhesives on etched dentine because of the increased bond strength compared with their application onto smear-layer-covered dentine, regardless of storage conditions.
authors.affiliation: Dental Clinic 1 -- Operative Dentistry and Periodontology, University of Erlangen, Erlangen, Germany.
authors.forename: Michael
authors.initials: M
authors.lastname: Taschner
authors.forename: Fernando
authors.initials: F
authors.lastname: Nato
authors.forename: Annalisa
authors.initials: A
authors.lastname: Mazzoni
authors.forename: Roland
authors.initials: R
authors.lastname: Frankenberger
authors.forename: Mirella
authors.initials: M
authors.lastname: Falconi
authors.forename: Anselm
authors.initials: A
authors.lastname: Petschelt
authors.forename: Lorenzo
authors.initials: L
authors.lastname: Breschi
mesh_terms: D001840:Dental Bonding / Q000379:methods*; D045662:Dental Etching / Q000379:methods*; D003763:Dental Leakage / Q000517:prevention & control*; D003784:Dental Pulp Calcification; D019232:Dental Restoration Failure; D003799:Dental Stress Analysis; D003804:Dentin / Q000187:drug effects*; D017220:Dentin-Bonding Agents / Q000627:therapeutic use*; D006801:Humans; D019279:Resin Cements / Q000627:therapeutic use; D013997:Time Factors
chemical_list: D017220:Dentin-Bonding Agents; D019279:Resin Cements