title: Bis(N-methyl-N-phenyl-carbamo-yl)disulfane.
abstract: The title compound, C(16)H(16)N(2)O(2)S(2), has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago. We now confirm the proposed mol-ecular structure in which the mol-ecule exhibits a twofold axis of symmetry through the mid-point of the S-S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].
authors.forename: Alayne L
authors.initials: AL
authors.lastname: Schroll
authors.forename: Maren
authors.initials: M
authors.lastname: Pink
authors.forename: George
authors.initials: G
authors.lastname: Barany