[Electrothermal atomic absorption determination of arsenic in plants and plant products].
The authors have developed the optimal temperature-time parameters of electrothermal atomic absorption determination of arsenic in plants after their acid predigestion. The matrix modifier is 1% nickel nitrate or palladium nitrate solution. Cuvettes (ovens) are simple, made of porous or pyrolytic graphite. The analytical program is suitable for both spectrometers with Zeeman and deuterium background correction. The correctness of the procedure has been estimated from the results of analysis of state reference samples certified for their arsenic content. The coefficient of variation was 20-35% for the concentration range of 0.02-0.2 mg/kg.
E A
EA
Karpova
A G
AG
Malysheva
A A
AA
Ermakov
N K
NK
Sidorenkova
D001151:Arsenic / Q000032:analysis*; D005504:Food Analysis / Q000295:instrumentation / Q000379:methods; D005506:Food Contamination / Q000032:analysis*; D057230:Limit of Detection; D010945:Plants, Edible / Q000737:chemistry*; D006109:Poaceae / Q000737:chemistry; D012015:Reference Standards; D012639:Seeds / Q000737:chemistry; D011198:Solanum tuberosum / Q000737:chemistry; D013054:Spectrophotometry, Atomic / Q000295:instrumentation / Q000379:methods*; D014908:Triticum / Q000737:chemistry
D001151:Arsenic