Resin-based composite light-cured properties assessed by laboratory standards and simulated clinical conditions.
SUMMARY The following parameters were varied: 1) irradiation technique: top and bottom polymerization according to the ISO standard, and polymerization from only the top, simulating clinical situations; 2) polymerization time: 5, 10, 20, and 40 seconds; 3) storage conditions: 24 hours in distilled water, thermocycling followed by storage for four weeks in artificial saliva or alcohol. Flexural strength (FS), flexural modulus (Eflexural), indentation modulus (E), Vickers hardness (HV), and degree of conversion (DC) were measured. The laboratory results were similar to those measured by mimicking clinical conditions only at high polymerization times and mild storage conditions (20 seconds and 40 seconds and storage for 24 hours in water, and 40 seconds with aging and storing in saliva). Significantly higher DC values were measured on the top than on the bottom of a 2-mm layer for all polymerization times. Overall, 5-second and 10-second irradiation times induced significantly lower DC values compared to the currently recommended polymerization times of 20 and 40 seconds at both the top and bottom of the samples. The initial DC differences as a function of irradiation time are leveled at 24 hours of storage but seem to do well in predicting long-term material behavior. A minimum irradiation time of 20 seconds is necessary clinically to achieve the best mechanical properties with modern high-intensity light emitting diode (LED) units.
Department of Restorative Dentistry, Ludwig-Maximilians University, Munich, Germany. nilie@dent.med.uni-muenchen.de
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Ilie
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Bauer
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Draenert
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Hickel
D017609:Barium Compounds / Q000737:chemistry; D017554:Carbon Compounds, Inorganic / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry*; D055117:Curing Lights, Dental / Q000145:classification; D003764:Dental Materials / Q000737:chemistry*; D003799:Dental Stress Analysis / Q000295:instrumentation; D055119:Elastic Modulus; D000431:Ethanol / Q000737:chemistry; D006244:Hardness; D006801:Humans; D055115:Light-Curing of Dental Adhesives / Q000295:instrumentation / Q000379:methods; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D053761:Nanocomposites / Q000737:chemistry; D018583:Pliability; D058105:Polymerization; D012464:Saliva, Artificial / Q000737:chemistry; D017655:Silicon Compounds / Q000737:chemistry; D012822:Silicon Dioxide / Q000737:chemistry; D012997:Solvents / Q000737:chemistry; D013314:Stress, Mechanical; D013499:Surface Properties; D013696:Temperature; D013997:Time Factors; D014867:Water / Q000737:chemistry; D015040:Zirconium / Q000737:chemistry
D017609:Barium Compounds; D017554:Carbon Compounds, Inorganic; D003188:Composite Resins; D003764:Dental Materials; D008689:Methacrylates; D012464:Saliva, Artificial; D017655:Silicon Compounds; D012997:Solvents; C102738:barium glass filler; D014867:Water; D000431:Ethanol; D012822:Silicon Dioxide; D015040:Zirconium; C028541:zirconium oxide; C022088:silicon carbide