title: Low solvothermal synthesis and characterization of hollow nanospheres molybdenum sulfide.
abstract: Hollow nanospheres of molybdenum disulfide have been synthesized by a novel solvothermal method under low temperature (180 degrees C). These nanomaterials were characterized by X-ray diffraction (XRD), Fourier transformation infra-red spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM, HRTEM) and X-ray Photoelectron Spectroscopy (XPS). A mechanism for the synthesis reaction is tentatively proposed and discussed.
authors.affiliation: Grupo de diseño molecular de catalizadores heterogéneos, Instituto de Catálisis y Petroleoquímica, UA UNED-ICP (CSIC), Campus de Cantoblanco, 28049 Madrid, Spain.
authors.forename: H
authors.initials: H
authors.lastname: Akram
authors.forename: C
authors.initials: C
authors.lastname: Mateos-Pedrero
authors.forename: E
authors.initials: E
authors.lastname: Gallegos-Suárez
authors.forename: N
authors.initials: N
authors.lastname: Allali
authors.forename: T
authors.initials: T
authors.lastname: Chafik
authors.forename: I
authors.initials: I
authors.lastname: Rodriguez-Ramos
authors.forename: A
authors.initials: A
authors.lastname: Guerrero Ruiz