title: Extraction and characterization of nanocellulose structures from raw cotton linter.
abstract: This study aimed to characterize nanocellulose extracted from cotton (Gossypium hirsutum) linters. The nanocellulose was subjected to electronic microscopy, thermal analysis, X-ray diffractometry, light scattering, and contact angle. The properties of the nanocellulose are considerably different from the linter. The acidic hydrolyses applied to extract the nanocrystals increased the crystallinity index and the hydrophilicity and decreased the thermal stability. On average, the nanocrystals were 177 nm long and 12 nm wide, with an aspect ratio of 19 when measured by microscopy. The light scattering results were coherent with the crystal dimensions. Cotton linter is a potential source of nanocellulose crystals, particularly to be used in the production of hydrophilic nanocomposites. Extraction of nanocellulose from raw cotton linter does not require pulping.
authors.affiliation: Embrapa Algodão, Rua Oswaldo Cruz, 1143, CEP 58428-095 Campina Grande, PB, Brazil. joao.morais@embrapa.br
authors.forename: João Paulo Saraiva
authors.initials: JP
authors.lastname: Morais
authors.forename: Morsyleide de Freitas
authors.initials: Mde F
authors.lastname: Rosa
authors.forename: Men de sá Moreira
authors.initials: Mde S
authors.lastname: de Souza Filho
authors.forename: Lidyane Dias
authors.initials: LD
authors.lastname: Nascimento
authors.forename: Diego Magalhães
authors.initials: DM
authors.lastname: do Nascimento
authors.forename: Ana Ribeiro
authors.initials: AR
authors.lastname: Cassales
mesh_terms: D002482:Cellulose / Q000737:chemistry* / Q000302:isolation & purification*; D032561:Cotton Fiber; D049329:Nanostructures / Q000737:chemistry*; D010316:Particle Size; D013696:Temperature
chemical_list: D002482:Cellulose