title: Microwave assisted synthesis of 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives using the complex cyanuric chloride/N,N-dimethylformamide.
abstract: A new and efficient method has been designed to prepare 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives by using the mixture of cyanuric chloride and N,N-dimethylformamide in a microwave-assisted reaction. The method used and presented here has good rate enhancement and excellent yields.
authors.affiliation: School of Chemical Science and Food Technology, Faculty of Science and Technology, University Kebangsaan Malaysia-UKM, Kuala Lumpur 43600, Malaysia. sm.shariat@yahoo.com
authors.forename: Mehdi
authors.initials: M
authors.lastname: Shariat
authors.forename: Mohd Wahid
authors.initials: MW
authors.lastname: Samsudin
authors.forename: Zuriati
authors.initials: Z
authors.lastname: Zakaria
mesh_terms: D048588:Benzoxazines / Q000138:chemical synthesis* / Q000737:chemistry; D004126:Dimethylformamide / Q000737:chemistry*; D008872:Microwaves; D044366:Transition Temperature; D014227:Triazines / Q000737:chemistry*; D062367:ortho-Aminobenzoates / Q000737:chemistry
chemical_list: D048588:Benzoxazines; D014227:Triazines; C579001:bis(4H-3,1-benzoxazin-4-one); D062367:ortho-Aminobenzoates; C031385:anthranilic acid; C019309:cyanuric chloride; D004126:Dimethylformamide