title: Influence of alloy microstructure on the microshear bond strength of basic alloys to a resin luting cement.
abstract: The aim of this study was to evaluate the influence of microstructure and composition of basic alloys on their microshear bond strength (µSBS) to resin luting cement. The alloys used were: Supreme Cast-V (SC), Tilite Star (TS), Wiron 99 (W9), VeraBond II (VBII), VeraBond (VB), Remanium (RM) and IPS d.SIGN 30 (IPS). Five wax patterns (13 mm in diameter and 4mm height) were invested, and cast in a centrifugal casting machine for each basic alloy. The specimens were embedded in resin, polished with a SiC paper and sandblasted. After cleaning the metal surfaces, six tygon tubes (0.5 mm height and 0.75 mm in diameter) were placed on each alloy surface, the resin cement (Panavia F) was inserted, and the excess was removed before light-curing. After storage (24 h/37°C), the specimens were subjected to µSBS testing (0.5 mm/min). The data were subjected to a one-way repeated measures analysis of variance and Turkey's test (α=0.05). After polishing, their microstructures were revealed with specific conditioners. The highest µSBS (mean/standard deviation in MPa) were observed in the alloys with dendritic structure, eutectic formation or precipitation: VB (30.6/1.7), TS (29.8/0.9), SC (30.6/1.7), with the exception of IPS (31.1/0.9) which showed high µSBS but no eutectic formation. The W9 (28.1/1.5), VBII (25.9/2.0) and RM (25.9/0.9) showed the lowest µSBS and no eutectic formation. It seems that alloys with eutectic formation provide the highest µSBS values when bonded to a light-cured resin luting cement.
authors.affiliation: Department of Dentistry I, Dental School, Federal University of Maranhão, São Luis, MA, Brazil. bauer@ufma.br
authors.forename: José
authors.initials: J
authors.lastname: Bauer
authors.forename: José Ferreira
authors.initials: JF
authors.lastname: Costa
authors.forename: Ceci Nunes
authors.initials: CN
authors.lastname: Carvalho
authors.forename: Douglas Nesadal de
authors.initials: DN
authors.lastname: Souza
authors.forename: Alessandro Dourado
authors.initials: AD
authors.lastname: Loguercio
authors.forename: Rosa Helena Miranda
authors.initials: RH
authors.lastname: Grande
mesh_terms: D000704:Analysis of Variance; D003722:Dental Alloys / Q000737:chemistry*; D001840:Dental Bonding / Q000379:methods*; D055115:Light-Curing of Dental Adhesives; D008422:Materials Testing / Q000379:methods*; D019279:Resin Cements / Q000737:chemistry*; D033081:Shear Strength
chemical_list: D003722:Dental Alloys; D019279:Resin Cements