title: [Not Available].
abstract: A sensitive and selective method using high-performance liquid chromatography in combination with atmospheric pressure chemical ionization tandem mass spetrometry (LC-APCI-MS/MS) has been developed for the determination of Deoxynivalenol (DON) in trace levels. The extract was purified with a MultiSep™ column followed by the Vicam™ DON immunoaffinity column. Quantification is based on an external standard method using positive Multiple Reaction Monitoring (MRM). The limit of detection was 5 μg/kg with a signal to noise ratio of 3:1.
authors.affiliation: Bundesinstitut für gesundheitlichen Verbraucherschutz und Veterinärmedizin, Thielallee 88-92, 14195, Berlin.
authors.forename: O
authors.initials: O
authors.lastname: Kappenstein
authors.forename: H St
authors.initials: HS
authors.lastname: Klaffke
authors.forename: Hj
authors.initials: H
authors.lastname: Spott
authors.forename: R
authors.initials: R
authors.lastname: Tiebach
authors.forename: R
authors.initials: R
authors.lastname: Weber