title: Everything SAXS: small-angle scattering pattern collection and correction.
abstract: For obtaining reliable nanostructural details of large amounts of sample--and if it is applicable--small-angle scattering (SAS) is a prime technique to use. It promises to obtain bulk-scale, statistically sound information on the morphological details of the nanostructure, and has thus led to many a researcher investing their time in it over the last eight decades of development. Due to pressure from scientists requesting more details on increasingly complex nanostructures, as well as the ever improving instrumentation leaving less margin for ambiguity, small-angle scattering methodologies have been evolving at a high pace over the past few decades. As the quality of any results can only be as good as the data that go into these methodologies, the improvements in data collection and all imaginable data correction steps are reviewed here. This work is intended to provide a comprehensive overview of all data corrections, to aid the small-angle scatterer to decide which are relevant for their measurement and how these corrections are performed. Clear mathematical descriptions of the corrections are provided where feasible. Furthermore, as no quality data exist without a decent estimate of their precision, the error estimation and propagation through all these steps are provided alongside the corrections. With these data corrections, the collected small-angle scattering pattern can be made of the highest standard, allowing for authoritative nanostructural characterization through its analysis. A brief background of small-angle scattering, the instrumentation developments over the years, and pitfalls that may be encountered upon data interpretation are provided as well.
authors.affiliation: International Center for Young Scientists, National Institute for Materials Science, 1-2-1 Sengen, 305-0047, Tsukuba, Japan. brian@stack.nl
authors.forename: Brian Richard
authors.initials: BR
authors.lastname: Pauw
mesh_terms: D053838:Scattering, Small Angle; D013223:Statistics as Topic; D014961:X-Ray Diffraction / Q000379:methods*