Recent developments in the synthetic chemistry of technetium disulfide.
Technetium disulfide was prepared by reaction between the elements in a sealed tube at 450 °C, by reaction between Tc2(O2CCH3)5 and H2S gas in a flowing system at 450 °C and by reaction between K2TcCl6 and H2S gas in sulfuric acid. The samples were analysed by X-ray absorption fine structure (XAFS) spectroscopy.
Department of Chemistry, University of Nevada Las Vegas, 4505 S. Maryland Parkway Box 454009, Las Vegas, NV 89154-4009, USA. maryline.ferrier@gmail.com.
Maryline
M
Ferrier
William M
WM
Kerlin
Frederic
F
Poineau
Alfred P
AP
Sattelberger
Kenneth R
KR
Czerwinski