title: Synthesis, structure and spectroscopic analyses of aquachloridooxidodiperoxidomolybdate(VI).
abstract: A novel aquachloridooxidodiperoxidomolybdate(vi), [MoClO(O2)2(OH2)](-), was crystallised as tetraethylammonium and triethylmethylammonium salts from strongly acidic aqueous solutions, and was structurally analysed by single crystal X-ray diffraction and NMR spectroscopy. The aqueous behaviour of the present anion observed by (17)O NMR agrees with that reported in a previous speciation study.
authors.affiliation: Department of Material Science and Chemistry, Faculty of Systems Engineering, Wakayama University, Sakaedani 930, Wakayama 640 8510, Japan. mh1043@center.wakayama-u.ac.jp.
authors.forename: Masa-aki
authors.initials: MA
authors.lastname: Saito
authors.forename: Masato
authors.initials: M
authors.lastname: Hashimoto