title: Spectroscopic (FT-IR, FT-Raman, 1H, 13C NMR, UV/VIS), thermogravimetric and antimicrobial studies of Ca(II), Mn(II), Cu(II), Zn(II) and Cd(II) complexes of ferulic acid.
abstract: The molecular structure of Mn(II), Cu(II), Zn(II), Cd(II) and Ca(II) ferulates (4-hydroxy-3-methoxycinnamates) was studied. The selected metal ferulates were synthesized. Their composition was established by means of elementary and thermogravimetric analysis. The following spectroscopic methods were used: infrared (FT-IR), Raman (FT-Raman), nuclear magnetic resonance ((13)C, (1)H NMR) and ultraviolet-visible (UV/VIS). On the basis of obtained results the electronic charge distribution in studied metal complexes in comparison with ferulic acid molecule was discussed. The microbiological study of ferulic acid and ferulates toward Escherichia coli, Bacillus subtilis, Candida albicans, Pseudomonas aeruginosa, Staphylococcus aureus and Proteus vulgaris was done.
authors: Division of Chemistry, Bialystok University of Technology, Zamenhofa 29, 15-435 Bialystok, Poland. Electronic address: m.kalinowska@pb.edu.pl.
authors: M
authors: M
authors: Kalinowska
authors: Division of Chemistry, Bialystok University of Technology, Zamenhofa 29, 15-435 Bialystok, Poland.
authors: J
authors: J
authors: Piekut
authors: University of Valenciennes and Hainaut-Cambrésis, Laboratoire des Matériaux Céramiques et Procédés Associés (LMCPA EA 2443), Le Mont Houy, 59313 Valenciennes, France.
authors: A
authors: A
authors: Bruss
authors: University of Valenciennes and Hainaut-Cambrésis, Laboratoire des Matériaux Céramiques et Procédés Associés (LMCPA EA 2443), Le Mont Houy, 59313 Valenciennes, France.
authors: C
authors: C
authors: Follet
authors: Department of General and Coordination Chemistry, Maria Curie-Skłodowska University, Lublin, Poland.
authors: J
authors: J
authors: Sienkiewicz-Gromiuk
authors: Division of Chemistry, Bialystok University of Technology, Zamenhofa 29, 15-435 Bialystok, Poland.
authors: R
authors: R
authors: Świsłocka
authors: Department of General and Coordination Chemistry, Maria Curie-Skłodowska University, Lublin, Poland.
authors: Z
authors: Z
authors: Rzączyńska
authors: Division of Chemistry, Bialystok University of Technology, Zamenhofa 29, 15-435 Bialystok, Poland. Electronic address: w-lewando@wp.pl.
authors: W
authors: W
authors: Lewandowski
mesh_terms: D000890:Anti-Infective Agents / Q000737:chemistry* / Q000494:pharmacology*; D001419:Bacteria / Q000187:drug effects; D002176:Candida albicans / Q000187:drug effects; D002177:Candidiasis / Q000188:drug therapy; D056831:Coordination Complexes / Q000737:chemistry* / Q000494:pharmacology*; D003373:Coumaric Acids / Q000737:chemistry* / Q000494:pharmacology*; D006801:Humans; D009682:Magnetic Resonance Spectroscopy; D013056:Spectrophotometry, Ultraviolet; D017550:Spectroscopy, Fourier Transform Infrared; D013059:Spectrum Analysis, Raman
chemical_list: D000890:Anti-Infective Agents; D056831:Coordination Complexes; D003373:Coumaric Acids; C004999:ferulic acid
keywords: (13)C and (1)H NMR; Antimicrobiological activity; FT-IR; FT-Raman; Metal 4-hydroxy-3-methoxycinnamates