title: High-throughput operando Raman-quadrupole mass spectrometer (QMS) system to screen catalytic systems.
abstract: This paper describes the design and setup of a high-throughput Raman system for an array of eight parallel catalytic reactors during reaction conditions. The "operando" methodology combines in situ spectroscopy during catalytic reaction with a simultaneous activity measurement. The high-throughput operando Raman system, multi-operando, is a device that automates this operando methodology for several catalyst samples at the same time, all samples being in the same reaction conditions. We describe how the system is made, how Raman system positions and acquires spectra, and how each reactor outlet gas is selected and analyzed.
authors.affiliation: Instituto de Catálisis y Petroleoquímica, CSIC, Marie Curie, 2; E-28049-Madrid, Spain.
authors.forename: Manuel
authors.initials: M
authors.lastname: García-Casado
authors.forename: José
authors.initials: J
authors.lastname: Prieto
authors.forename: Emilio
authors.initials: E
authors.lastname: Vico-Ruiz
authors.forename: Enrique
authors.initials: E
authors.lastname: Lozano-Diz
authors.forename: Consuelo
authors.initials: C
authors.lastname: Goberna-Selma
authors.forename: Miguel A
authors.initials: MA
authors.lastname: Bañares