One-minute synthesis of crystalline microporous aluminophosphate (AlPO4-5) by combining fast heating with a seed-assisted method.
Herein, we report a rapid route for the synthesis of AlPO4-5. By combining fast heating in a tubular reactor with a seed-assisted method, both of which were found to be crucial, the preparation of AlPO4-5 was completed in one minute, making this route the fastest known for the preparation of the crystalline microporous materials.
Department of Chemical System Engineering, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-8656, Japan. okubo@chemsys.t.u-tokyo.ac.jp.
Zhendong
Z
Liu
Toru
T
Wakihara
Daisuke
D
Nishioka
Kazunori
K
Oshima
Takahiko
T
Takewaki
Tatsuya
T
Okubo