title: Investigation on diazinon and oxydemeton-methyl residues in cucumbers grown in Kerman greenhouses.
abstract: Pesticides are considered as the most polluting substances. The residue of pesticides in agricultural crops, especially in greenhouse harvests, has been reported critical. Cucumber, considered as a vegetable, is an agricultural product which is commonly found in the Iranian food basket. The current study aims to assess the level of diazinon and oxydemeton-methyl existing in cucumbers sampled from Kerman greenhouses. The pesticide residue was extracted by acetone and dichloromethane. The extracts were cleaned up according to the solid-phase extraction method. The pesticide residues were then determined by capillary gas chromatography with nitrogen-phosphorus detection. The recoveries were 83 and 85 %, the limit of detection was 0.028 and 0.034 mg/kg, and the limits of qualification were 0.093 and 0.113 mg/kg for diazinon and oxydemeton-methyl in cucumber samples, respectively. The median of diazinon residue was detected 0.582 mg/kg, which was 11.64 times the national maximum residue limit (MRL) (0.05 mg/kg), and the median for oxydemeton-methyl was 1.910 mg/kg, being 1.91 times the MRL (1 mg/kg).
authors: Department of Plant Protection, Kerman's Agricultural and Natural Resources Research Center, Kerman, 7617913739, Iran, f.ganjei@yahoo.com.
authors: Fatemeh
authors: F
authors: Ganjeizadeh Rohani
authors: Vahideh
authors: V
authors: Mahdavi
authors: M Mehdi
authors: MM
authors: Aminaei
mesh_terms: D018553:Cucumis sativus / Q000737:chemistry* / Q000254:growth & development; D003976:Diazinon / Q000032:analysis*; D004784:Environmental Monitoring; D009946:Organothiophosphorus Compounds / Q000032:analysis*; D010573:Pesticide Residues / Q000032:analysis*; D052616:Solid Phase Extraction
chemical_list: D009946:Organothiophosphorus Compounds; D010573:Pesticide Residues; C026086:methyl demeton; D003976:Diazinon