title: [Evaluation of the methods for the determination of nitrites in baby foods according Mexican legislation].
abstract: We evaluated the two methods accepted by the Mexican norm for the determination of nitritesin infant meat-based food with vegetables. We determined the content of nitrites in the infant food, raw materials as well as products from the intermediate stages of production. A reagent blank and a reference sample were included at each analytical run. In addition, we determined the sensitivity, recovery percentage and accuracy of each methodology. Infant food results indicated an important difference in the nitrite content determined under each methodology, due to the persistent presence of turbidity in the extracts. Different treatments were proposed to eliminate the turbidity, but these only managed to reduce it. The turbidity was attributed to carbohydrates which disclosed concentration exhibit a wide dispersion and were below the quantifiable limit under both methodologies; therefore it is not recommended to apply these techniques with food suspected to contain traces of nitrites.
authors.forename: Josefina C
authors.initials: JC
authors.lastname: Morales Guerrero
authors.forename: Rodrigo A
authors.initials: RA
authors.lastname: García Zepeda
authors.forename: Edgar
authors.initials: E
authors.lastname: Flores Ruvalcaba
authors.forename: Lorelei
authors.initials: L
authors.lastname: Martínez Michel
mesh_terms: D005504:Food Analysis / Q000331:legislation & jurisprudence / Q000379:methods; D006801:Humans; D007223:Infant; D007225:Infant Food / Q000032:analysis* / Q000592:standards; D008800:Mexico; D009573:Nitrites / Q000032:analysis*
chemical_list: D009573:Nitrites