title: A convenient semisynthesis of myricetin-3-O-β-d-glucuronide.
abstract: Myricetin-3-O-β-d-glucuronide, a bioactive flavonol glycoside, was synthesized effectively starting from myricetrin in a total yield of 49.2%. The structures of all synthetic compounds were confirmed by (1)H, (13)C NMR, and HR-MS techniques.
authors.affiliation: a State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Key Laboratory of Biosynthesis of Natural Products, Ministry of Health of PRC, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College , Beijing 100050 , China.
authors.forename: Hong-Lin
authors.initials: HL
authors.lastname: Wu
authors.forename: Yuan-Feng
authors.initials: YF
authors.lastname: Tong
authors.forename: Song
authors.initials: S
authors.lastname: Wu
mesh_terms: D005419:Flavonoids / Q000138:chemical synthesis* / Q000737:chemistry; D044948:Flavonols / Q000737:chemistry; D020719:Glucuronides / Q000138:chemical synthesis* / Q000737:chemistry; D015394:Molecular Structure; D019906:Nuclear Magnetic Resonance, Biomolecular; D013237:Stereoisomerism
chemical_list: D005419:Flavonoids; D044948:Flavonols; D020719:Glucuronides; C040015:myricetin; C072578:myricetin 3-O-glucuronide
keywords: 3′,4′,5′,5,7-penta-O-benzylmyricetin; myricetin-3-O-β-d-glucuronide; semisynthesis