title: Synthesis, crystal growth and spectroscopic investigation of novel metal organic crystal: β-alanine cadmium bromide monohydrate (β-ACBM).
abstract: β-Alanine cadmium bromide monohydrate (β-ACBM), a new metal organic crystal has been grown from aqueous solution by slow evaporation technique. The grown crystals have been subjected to single crystal X-ray diffraction analysis to determine the crystal structure. The β-ACBM crystallized in monoclinic system with space group P2(1)/c. The presence of protons and carbons in the β-alanine cadmium bromide monohydrate was confirmed by (1)H and (13)C nuclear magnetic resonance spectral analysis. The mode of vibration of different molecular groups present in β-ACBM was identified by FT-IR spectral analysis. Transparency of crystals in UV-Vis-NIR region has also been studied. The thermal characteristics of as-grown crystals were analyzed using thermo gravimetric and differential thermal analyses. The magnetic property of the grown crystal was investigated using Vibrating Sample Magnetometer (VSM) at ambient temperature. The mechanical stability of β-ACBM was evaluated by Vickers microhardness measurement.
authors.affiliation: Department of Physics, SriGuru Institute of Technology, Coimbatore 641110, India.
authors.forename: R
authors.initials: R
authors.lastname: Renugadevi
authors.affiliation: Department of Physics, Sri Ramakrishna Engineering College, Coimbatore 641020, India. Electronic address: kesav_cbe@yahoo.co.in.
authors.forename: R
authors.initials: R
authors.lastname: Kesavasamy
mesh_terms: D000409:Alanine / Q000737:chemistry*; D001965:Bromides / Q000737:chemistry*; D019187:Cadmium Compounds / Q000138:chemical synthesis* / Q000737:chemistry*; D003460:Crystallization; D018360:Crystallography, X-Ray; D013053:Spectrophotometry
chemical_list: D001965:Bromides; D019187:Cadmium Compounds; D000409:Alanine
keywords: Chemical synthesis; Crystal growth; Crystal structure; Magnetic materials; Molecular structure