N-(2-Chloro-eth-yl)morpholine-4-carbox-amide.
The title compound, C7H13ClN2O2, synthesized by the reaction of 2-chloro-ethyl iso-cyanate and morpholine, crystallizes with four molecules in the asymmetric unit, which have similar conformations and comprise two pairs each related by approximate non-crystallographic inversion centres. Two of them have a modest orientational disorder of the 2-chloro-ethyl fragments [occupancy ratio of 0.778 (4):0.222 (4)]. In the crystal, mol-ecules are linked by N-H⋯O=C hydrogen bonds, forming three crystallographically different kinds of infinite hydrogen-bonded chains extending along [001].
Department of Pure and Industrial Chemistry, University of Nigeria, Nsukka, Enugu State, Nigeria.
Oguejiofo T
OT
Ujam
Department of Pure and Industrial Chemistry, University of Nigeria, Nsukka, Enugu State, Nigeria.
Jonnie N
JN
Asegbeloyin
Department of Chemistry, University of Waikato, Private Bag 3105, Hamilton, New Zealand.
Brian K
BK
Nicholson
Department of Pure and Industrial Chemistry, University of Nigeria, Nsukka, Enugu State, Nigeria.
Pius O
PO
Ukoha
Department of Pure and Industrial Chemistry, University of Nigeria, Nsukka, Enugu State, Nigeria.
Nkechi N
NN
Ukwueze