title: Implementation of focused ion beam (FIB) system in characterization of nuclear fuels and materials.
abstract: Beginning in 2007, a program was established at the Idaho National Laboratory to update key capabilities enabling microstructural and micro-chemical characterization of highly irradiated and/or radiologically contaminated nuclear fuels and materials at scales that previously had not been achieved for these types of materials. Such materials typically cannot be contact handled and pose unique hazards to instrument operators, facilities, and associated personnel. Over the ensuing years, techniques have been developed and operational experience gained that has enabled significant advancement in the ability to characterize a variety of fuel types including metallic, ceramic, and coated particle fuels, obtaining insights into in-reactor degradation phenomena not achievable by any other means. The following article describes insights gained, challenges encountered, and provides examples of unique results obtained in adapting dual beam FIB technology to nuclear fuels characterization.
authors: Idaho National Laboratory, Idaho Falls, ID 83415, United States. Electronic address: assel.aitkaliyeva@inl.gov.
authors: A
authors: A
authors: Aitkaliyeva
authors: Idaho National Laboratory, Idaho Falls, ID 83415, United States.
authors: J W
authors: JW
authors: Madden
authors: Idaho National Laboratory, Idaho Falls, ID 83415, United States.
authors: B D
authors: BD
authors: Miller
authors: Idaho National Laboratory, Idaho Falls, ID 83415, United States.
authors: J I
authors: JI
authors: Cole
keywords: Contamination; Focused ion beam (FIB); Nuclear materials; Radioactivity