title: Fast method for synthesis of alkyl and aryl-N-methylnitrones.
abstract: A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.
authors.affiliation: Chemistry Department, Faculty of Science, Gazi University, Ankara 06500, Turkey.
authors.forename: Serkan
authors.initials: S
authors.lastname: Yavuz
authors.affiliation: Chemistry Department, Faculty of Science, Çankırı Karatekin University, Çankırı 18100, Turkey.
authors.forename: Hamdi
authors.initials: H
authors.lastname: Ozkan
authors.affiliation: Chemistry Department, Faculty of Science and Arts, Hitit University, Çorum 19030, Turkey.
authors.forename: Naki
authors.initials: N
authors.lastname: Colak
authors.affiliation: Chemistry Department, Faculty of Science, Gazi University, Ankara 06500, Turkey. yildirir@gazi.edu.tr.
authors.forename: Yilmaz
authors.initials: Y
authors.lastname: Yildirir
mesh_terms: D002625:Chemistry, Organic / Q000379:methods*; D009589:Nitrogen Oxides / Q000138:chemical synthesis* / Q000737:chemistry; D066244:Proton Magnetic Resonance Spectroscopy; D013997:Time Factors; D044366:Transition Temperature
chemical_list: D009589:Nitrogen Oxides; C015388:nitrones