title: Multi-residue determination of eleven anticoagulant rodenticides by high-performance liquid chromatography with diode array/fluorimetric detection: investigation of suspected animal poisoning in the period 2012-2013 in north-eastern Italy.
abstract: Misuse or deliberate abuse of anticoagulant rodenticides (AR) may often result in incidental or malicious non-target animal poisoning. This study presents preliminary results of the analysis of 561 real suspected samples, ranging from baits to livers and stomach contents, collected at the Istituto Zooprofilattico Sperimentale delle Venezie (official referral laboratory for the regions of north-eastern Italy), in the period 2012-2013. Samples were analyzed by a method based on a combination of liquid chromatography with diode array/fluorescence detection (HPLC-DAD/F) able to identify 11 different AR (brodifacoum, bromadiolone, chloropahacinone, coumachlor, coumafuryl, coumatetralyl, difenacoum, diphacinone, flocoumafen, pindone, warfarin).
authors.affiliation: Istituto Zooprofilattico Sperimentale delle Venezie, Chemistry Department, viale dell'Università 10, 35020 Legnaro, Padova, Italy. Electronic address: fgallocchio@izsvenezie.it.
authors.forename: Federica
authors.initials: F
authors.lastname: Gallocchio
authors.affiliation: Istituto Zooprofilattico Sperimentale delle Venezie, Chemistry Department, viale dell'Università 10, 35020 Legnaro, Padova, Italy.
authors.forename: Lara
authors.initials: L
authors.lastname: Basilicata
authors.affiliation: Istituto Zooprofilattico Sperimentale delle Venezie, Chemistry Department, viale dell'Università 10, 35020 Legnaro, Padova, Italy.
authors.forename: Cristiana
authors.initials: C
authors.lastname: Benetti
authors.affiliation: Istituto Zooprofilattico Sperimentale delle Venezie, Chemistry Department, viale dell'Università 10, 35020 Legnaro, Padova, Italy.
authors.forename: Roberto
authors.initials: R
authors.lastname: Angeletti
authors.affiliation: Istituto Zooprofilattico Sperimentale delle Venezie, Chemistry Department, viale dell'Università 10, 35020 Legnaro, Padova, Italy.
authors.forename: Giovanni
authors.initials: G
authors.lastname: Binato
mesh_terms: D000818:Animals; D000925:Anticoagulants / Q000032:analysis* / Q000506:poisoning*; D002853:Chromatography, Liquid; D005470:Fluorometry; D005766:Gastrointestinal Contents / Q000737:chemistry; D007558:Italy; D008099:Liver / Q000737:chemistry; D012378:Rodenticides / Q000032:analysis* / Q000506:poisoning*
chemical_list: D000925:Anticoagulants; D012378:Rodenticides
keywords: Animal poisoning; Anticoagulant rodenticides; HPLC-DAD/F