title: High aspect ratio AFM Probe processing by helium-ion-beam induced deposition.
abstract: A Scanning Helium Ion Microscope (SHIM) is a high resolution surface observation instrument similar to a Scanning Electron Microscope (SEM) since both instruments employ finely focused particle beams of ions or electrons [1]. The apparent difference is that SHIMs can be used not only for a sub-nanometer scale resolution microscopic research, but also for the applications of very fine fabrication and direct lithography of surfaces at the nanoscale dimensions. On the other hand, atomic force microscope (AFM) is another type of high resolution microscopy which can measure a three-dimensional surface morphology by tracing a fine probe with a sharp tip apex on a specimen's surface.In order to measure highly uneven and concavo-convex surfaces by AFM, the probe of a high aspect ratio with a sharp tip is much more necessary than the probe of a general quadrangular pyramid shape. In this paper we report the manufacture of the probe tip of the high aspect ratio by ion-beam induced gas deposition using a nanoscale helium ion beam of SHIM.Gas of platinum organic compound was injected into the sample surface neighborhood in the vacuum chamber of SHIM. The decomposition of the gas and the precipitation of the involved metal brought up a platinum nano-object in a pillar shape on the normal commercial AFM probe tip. A SHIM system (Carl Zeiss, Orion Plus) equipped with the gas injection system (OmniProbe, OmniGIS) was used for the research. While the vacuum being kept to work, we injected platinum organic compound ((CH3)3(CH3C5H4)Pt) into the sample neighborhood and irradiated the helium ion beam with the shape of a point on the apex of the AFM probe tip. It is found that we can control the length of the Pt nano-pillar by irradiation time of the helium ion beam. The AFM probe which brought up a Pt nano-pillar is shown in Figure 1. It is revealed that a high-aspect-ratio Pt nano-pillar of ∼40nm diameter and up to ∼2000 nm length can be grown. In addition, for possible heating by the helium ion beam, it was observed that an original probe shape was transformed. AFM measurement of a reference sample (pitch 100-500 nm, depth 100 nm) of the lines and spaces was performed using the above probes. The conventional probes which did not bring up platinum was not able to get into the ditch enough. Therefore it was found that a salient was big and a reentrant was shallow. On the other hand, the probe which brought up platinum was able to enter enough to the depths of the ditch.jmicro;63/suppl_1/i30-a/DFU075F1F1DFU075F1Fig.1.SHIM image of the AFM probe with the Pt nano-pillar fabricated by ion-beam induced deposition.
authors.affiliation: Surface Characterization Group, Nano Characterization Unit, Advanced Key Technologies Division, National Institute for Materials Science.
authors.forename: Keiko
authors.initials: K
authors.lastname: Onishi
authors.affiliation: Nano Interface Characterization Group, Nano-interface Characterization Field, Global Research Center for Environment and Energy based on Nanomaterials Science, National Institute for Materials Science 1-2-1 Sengen, Tsukuba, Ibaraki, Japan.
authors.forename: Hongxuan
authors.initials: H
authors.lastname: Guo
authors.affiliation: Surface Characterization Group, Nano Characterization Unit, Advanced Key Technologies Division, National Institute for Materials Science.
authors.forename: Syoko
authors.initials: S
authors.lastname: Nagano
authors.affiliation: Surface Characterization Group, Nano Characterization Unit, Advanced Key Technologies Division, National Institute for Materials Science Nano Interface Characterization Group, Nano-interface Characterization Field, Global Research Center for Environment and Energy based on Nanomaterials Science, National Institute for Materials Science 1-2-1 Sengen, Tsukuba, Ibaraki, Japan.
authors.forename: Daisuke
authors.initials: D
authors.lastname: Fujita