title: Rapid bonding and easy debonding of orthodontic appliances with 4-META/MMA-TBB resin using thermal heating.
abstract: 4-Methacryloyloxyethyl trimellitate anhydride/methyl methacrylate-tri-n-butylborane (4-META/MMA-TBB) resin is widely used as a direct bonding adhesive for orthodontic appliances because of its strong bonding ability. However, its clinical disadvantages include long setting times and difficult debonding with subsequent residual adhesive left on the enamel surface. To resolve these problems, thermal heating was applied to orthodontic appliances. The setting time was dramatically reduced by thermal heating (160°C for 5 s), with the shear bond strength remaining the same as that stated in the manufacturer's instructions. Debonding of appliances following thermal heating (160°C for 20 s) could be easily performed, decreasing the amount of adhesive left on enamel. These conditions were not accompanied by an increase in the heat pain threshold of pulpal dentin. These results suggest that the use of thermal heating in the bonding/debonding of 4-META/MMA-TBB resin may resolve its clinical weaknesses, making its ease of use similar to light-cured resin.
authors.affiliation: Department of Orthodontics, Nippon Dental University, School of Life Dentistry at Niigata.
authors.forename: Takashi
authors.initials: T
authors.lastname: Kameda
authors.forename: Kazuo
authors.initials: K
authors.lastname: Ohkuma
authors.forename: Kazuto
authors.initials: K
authors.lastname: Terada
mesh_terms: D000818:Animals; D001896:Boron Compounds / Q000737:chemistry*; D002417:Cattle; D001840:Dental Bonding / Q000379:methods*; D017005:Dental Debonding / Q000379:methods*; D006358:Hot Temperature; D066298:In Vitro Techniques; D007180:Incisor; D008689:Methacrylates / Q000737:chemistry*; D008768:Methylmethacrylates / Q000737:chemistry*; D016910:Orthodontic Brackets; D033081:Shear Strength
chemical_list: D001896:Boron Compounds; D008689:Methacrylates; D008768:Methylmethacrylates; C476987:methylmethacrylate-tributylborane resin; C034139:4-methacryloxyethyltrimellitic acid anhydride; C049495:Super-bond