title: [Analysis of pesticides in blood specimen by GC/MS with accelerated solvent extraction].
abstract: OBJECTIVE
  To develop the accelerated solvent extraction (ASE) for determining pesticides present in blood samples.
  
  
  METHODS
  Pesticides were extracted by ASE with optimized parameters to study recovery rate affected by extraction temperature, time and agent. GC/MS was used to perform quantitative analysis.
  
  
  RESULTS
  The recovery rates of eight pesticides were 70.6%-92.4%. The coefficient of variation was less than 5.0%. A good linear relationship was obtained at the concentration range of 0.5-5.0 microg/mL.
  
  
  CONCLUSIONS
  The method was fast and simple with high recovery rate and good repeatability. It can be applied to analyze pesticides present in the blood specimen.
authors: Wen-hai
authors: WH
authors: Li
authors: Da-wei
authors: DW
authors: Lin
authors: Hong-lei
authors: HL
authors: Sun
authors: Maimaitituxun
authors: M
authors: Mutailifu
authors: Lei
authors: L
authors: Wang
mesh_terms: D002853:Chromatography, Liquid; D008401:Gas Chromatography-Mass Spectrometry; D010575:Pesticides / Q000097:blood*; D012997:Solvents; D013696:Temperature; D013997:Time Factors
chemical_list: D010575:Pesticides; D012997:Solvents