title: Headspace solid-phase microextraction for wine volatile analysis.
abstract: The most commonly used technique to prepare samples for the analysis of wine volatile is the headspace solid-phase microextraction (HS-SPME). This method has gained popularity in last few years, as it is a unique solventless preparation technique. In this paper, a summary of recently published studies using HS-SPME for the analysis of wine aromas, with special emphasis on the method developed, has been compiled. Several papers are discussed in detail, mainly with respect to the SPME conditions used. A brief summary of the reviews related to HS-SPME analysis is given and discussed. Several parameters affecting the HS-SPME, such as the salt concentration and the agitation conditions, are used in the same way as used in several papers. The HS-SPME extraction proved to be sufficiently sensitive to satisfy legislative requirements related to low detection and quantification limits as well as method accuracy and precision requirements. However, in order to achieve the best performance and precision, the protocol needs to be optimized for each case. The effect of different parameters must be well characterized to ensure correct extraction and desorption to ensure the transfer of extracted compounds into the analytical system. The operating parameters, such as time, temperature, and agitation, must then be kept constant for all the samples.
authors.affiliation: a Faculty of Agricultural and Food Sciences , Holy Spirit University of Kaslik (USEK) , Jounieh , Lebanon.
authors.forename: Samar
authors.initials: S
authors.lastname: Azzi-Achkouty
authors.affiliation: b Department of Chemistry and Life Sciences , Higher Center of Research (CSR), Holy Spirit University of Kaslik (USEK) , Jounieh , Lebanon.
authors.forename: Nathalie
authors.initials: N
authors.lastname: Estephan
authors.affiliation: b Department of Chemistry and Life Sciences , Higher Center of Research (CSR), Holy Spirit University of Kaslik (USEK) , Jounieh , Lebanon.
authors.forename: Naïm
authors.initials: N
authors.lastname: Ouaini
authors.affiliation: c AgroParisTech/INRA , UMR1145 Ingénierie Procédés Aliments , Paris , France.
authors.forename: Douglas N
authors.initials: DN
authors.lastname: Rutledge
mesh_terms: D053000:Analytic Sample Preparation Methods; D005513:Food Inspection / Q000379:methods* / Q000592:standards / Q000639:trends; D063427:Food Quality; D009812:Odorants; D011786:Quality Control; D015203:Reproducibility of Results; D052617:Solid Phase Microextraction; D013457:Sulfur Compounds / Q000032:analysis; D055549:Volatile Organic Compounds / Q000032:analysis*; D014835:Volatilization; D014920:Wine / Q000032:analysis*
chemical_list: D013457:Sulfur Compounds; D055549:Volatile Organic Compounds
keywords: HS-SPME; aroma; volatile; wine