title: [THE DEVELOPMENT AND VALIDATION OF THE GAS CHROMATOGRAPHY METHOD AND VALIDATION DEVELOPMENT FOR THE ORGANIC CYANIDE (CYANOETHYLENE) DETERMINATION IN EXPIRED AIR].
abstract: There are presented results of experimental studies on the development of gas chromatography method for the cyan ethylene determination in expired air During the process of the study there was chosen and proved the capillary gas chromatography method; there were investigated and elaborated optimal parameters of the gas chromatography separation of cyanoethylene with associated hydrocarbons together with the sample preparation and quantitative measurement methods. There was achieved the optimal level of gas chromatography quantification method for the cyan ethylene determination at 0, 00012 mg/m3, with the method uncertainty not more than 25%. The method was tried during the medical and biological examination of groups of 6-8 years old children, living in the territory of exposition from the moment of the birth and in the control territory.
authors: N V
authors: NV
authors: Zaĭtseva
authors: T S
authors: TS
authors: Ulanova
authors: T V
authors: TV
authors: Nurislamova
authors: N A
authors: NA
authors: Popova
authors: O A
authors: OA
authors: Mal'tseva
mesh_terms: D000388:Air / Q000032:analysis*; D003486:Cyanides / Q000032:analysis*; D045853:Exhalation; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods*; D006801:Humans; D015203:Reproducibility of Results
chemical_list: D003486:Cyanides