title: Probing structural and motional features of organic and inorganic solids through extended family of cross-polarization experiments.
abstract: Combined use of cross-polarization and magic-angle spinning in the middle of the seventies has opened a new era of high-resolution solid-state NMR spectroscopy. Cross-polarization procedure is commonly used to obtain a shorter measuring time and to investigate or exploit one nucleous by means of the other nucleous involved in the polarization transfer. An extended family of cross-polarization experiments including constant time cross-polarization approach, cross-polarization inversion and indirect observation of proton spin system is reviewed and illustrated with applications to a large range of solids.
authors.affiliation: École Normale Supérieure-PSL Research University, Sorbonne Universités-UPMC University, CNRS, UMR 7203 LBM, Paris, France. Electronic address: Piotr.Tekely@ens.fr.
authors.forename: Piotr
authors.initials: P
authors.lastname: Tekely
keywords: Constant-time cross-polarization; Cross-polarization; Cross-polarization inversion; Magic-angle spinning; Magnetization transfer; Solid-state NMR