title: 1020MHz single-channel proton fast magic angle spinning solid-state NMR spectroscopy.
abstract: This study reports a first successful demonstration of a single channel proton 3D and 2D high-throughput ultrafast magic angle spinning (MAS) solid-state NMR techniques in an ultra-high magnetic field (1020MHz) NMR spectrometer comprised of HTS/LTS magnet. High spectral resolution is well demonstrated.
authors.affiliation: RIKEN CLST-JEOL Collaboration Center, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Manoj Kumar
authors.initials: MK
authors.lastname: Pandey
authors.affiliation: Biophysics and Department of Chemistry, The University of Michigan, Ann Arbor, MI 48109-1055, USA.
authors.forename: Rongchun
authors.initials: R
authors.lastname: Zhang
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Kenjiro
authors.initials: K
authors.lastname: Hashi
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Shinobu
authors.initials: S
authors.lastname: Ohki
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Gen
authors.initials: G
authors.lastname: Nishijima
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Shinji
authors.initials: S
authors.lastname: Matsumoto
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Takashi
authors.initials: T
authors.lastname: Noguchi
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Kenzo
authors.initials: K
authors.lastname: Deguchi
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Atsushi
authors.initials: A
authors.lastname: Goto
authors.affiliation: National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan.
authors.forename: Tadashi
authors.initials: T
authors.lastname: Shimizu
authors.affiliation: Center for Life Science Technologies, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Hideaki
authors.initials: H
authors.lastname: Maeda
authors.affiliation: Center for Life Science Technologies, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Masato
authors.initials: M
authors.lastname: Takahashi
authors.affiliation: Center for Life Science Technologies, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Yoshinori
authors.initials: Y
authors.lastname: Yanagisawa
authors.affiliation: Center for Life Science Technologies, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Toshio
authors.initials: T
authors.lastname: Yamazaki
authors.affiliation: Center for Life Science Technologies, RIKEN, Yokohama, Kanagawa 230-0045, Japan.
authors.forename: Seiya
authors.initials: S
authors.lastname: Iguchi
authors.affiliation: JEOL RESONANCE Inc., Akishima, Tokyo 196-8558, Japan.
authors.forename: Ryoji
authors.initials: R
authors.lastname: Tanaka
authors.affiliation: JEOL RESONANCE Inc., Akishima, Tokyo 196-8558, Japan.
authors.forename: Takahiro
authors.initials: T
authors.lastname: Nemoto
authors.affiliation: JEOL RESONANCE Inc., Akishima, Tokyo 196-8558, Japan.
authors.forename: Tetsuo
authors.initials: T
authors.lastname: Miyamoto
authors.affiliation: JEOL RESONANCE Inc., Akishima, Tokyo 196-8558, Japan.
authors.forename: Hiroto
authors.initials: H
authors.lastname: Suematsu
authors.affiliation: Kobe Steel Ltd., Kobe, Hyogo 651-2271, Japan.
authors.forename: Kazuyoshi
authors.initials: K
authors.lastname: Saito
authors.affiliation: Kobe Steel Ltd., Kobe, Hyogo 651-2271, Japan.
authors.forename: Takashi
authors.initials: T
authors.lastname: Miki
authors.affiliation: Biophysics and Department of Chemistry, The University of Michigan, Ann Arbor, MI 48109-1055, USA. Electronic address: ramamoor@umich.edu.
authors.forename: Ayyalusamy
authors.initials: A
authors.lastname: Ramamoorthy
authors.affiliation: RIKEN CLST-JEOL Collaboration Center, RIKEN, Yokohama, Kanagawa 230-0045, Japan; JEOL RESONANCE Inc., Akishima, Tokyo 196-8558, Japan. Electronic address: yunishiy@jeol.co.jp.
authors.forename: Yusuke
authors.initials: Y
authors.lastname: Nishiyama
mesh_terms: D004574:Electromagnetic Fields; D006639:Histidine / Q000737:chemistry; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000379:methods; D011522:Protons; D014443:Tyrosine / Q000737:chemistry
chemical_list: D011522:Protons; D014443:Tyrosine; D006639:Histidine
keywords: Proton detection; Solid-state NMR; Structure elucidation; Ultra-high field; Ultrafast MAS