title: Crystal structure of 5,5'-bis-(di-methyl-amino)-N,N'-(3-methyl-3-aza-pentane-1,5-di-yl)di(naphthalene-1-sulfonamide).
abstract: In the title compound, C29H37N5O4S2, two arms substituted with dansyl derivatives are connected to a central tertiary amine, where the dihedral angle between the planes of two dansyl units is 56.39 (4)°. Each arm contains a sulfonamide functional group and both N-H groups in the compound are pointed to the same side. The central part of the mol-ecule is disordered over three sets of sites with a refined occupancy ratio of 0.547 (4):0.328 (4):0.125 (3). No intra-molecular π-π or hydrogen-bonding inter-actions are observed. In the crystal, mol-ecules are linked via pairs of N-H⋯O inter-actions involving the same acceptor atom, forming inversion dimers. In addition, C-H⋯O inter-actions exist between molecules, providing further stabilization of dimers.
authors: Department of Chemistry and Biochemistry, Jackson State University, Jackson, MS 39217, USA.
authors: Toyketa V
authors: TV
authors: Horne
authors: Department of Chemistry and Biochemistry, Jackson State University, Jackson, MS 39217, USA.
authors: Syed A
authors: SA
authors: Haque
authors: Department of Chemistry and Biochemistry, Jackson State University, Jackson, MS 39217, USA.
authors: Adrianne
authors: A
authors: Barton
authors: Department of Chemistry and Biochemistry, Jackson State University, Jackson, MS 39217, USA.
authors: Md Alamgir
authors: MA
authors: Hossain
keywords: crystal structure; dansyl derivative; hydrogen bonding; sulfonamide