title: Thermal analysis, X-ray powder diffraction and electron microscopy data related with the production of 1:1 Caffeine:Glutaric Acid cocrystals.
abstract: The data presented in this article are related to the production of 1:1 Caffeine:Glutaric Acid cocrystals as part of the research article entitled "Green production of cocrystals using a new solvent-free approach by spray congealing" (Duarte et al., 2016) [1]. More specifically, here we present the thermal analysis and the X-ray powder diffraction data for pure Glutaric Acid, used as a raw material in [1]. We also include the X-ray powder diffraction and electron microscopy data obtained for the 1:1 Caffeine:Glutaric Acid cocrystal (form II) produced using the cooling crystallization method reported in "Operating Regions in Cooling Cocrystallization of Caffeine and Glutaric Acid in Acetonitrile" (Yu et al., 2010) [2]. Lastly, we show the X-ray powder diffraction data obtained for assessing the purity of the 1:1 Caffeine:Glutaric cocrystals produced in [1].
authors.affiliation: Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa, Lisbon, Portugal; R&D Drug Product Development, Hovione Farmaciência SA, Loures, Portugal.
authors.forename: Íris
authors.initials: Í
authors.lastname: Duarte
authors.affiliation: R&D Drug Product Development, Hovione Farmaciência SA, Loures, Portugal.
authors.forename: Rita
authors.initials: R
authors.lastname: Andrade
authors.affiliation: Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa, Lisbon, Portugal.
authors.forename: João F
authors.initials: JF
authors.lastname: Pinto
authors.affiliation: R&D Drug Product Development, Hovione Farmaciência SA, Loures, Portugal.
authors.forename: Márcio
authors.initials: M
authors.lastname: Temtem