title: Fast analysis of volatile compounds from Lippia citriodora with nanoporous aluminum wire as solid-phase microextraction fibres.
abstract: In this study, the efficiency of nanoporous aluminium wires as fibres for headspace solid-phase microextraction (HS-SPME) of volatile compounds from Lippia citriodora was investigated and compared with two anodised methods. The prepared fibres are durable with very good chemical and thermal stability which can be coupled to GC and GC/MS. A one at-a-time optimisation strategy was applied for optimising the important extraction parameters such as extraction temperature, extraction time, sample mass and added water. Compared with hydrodistillation (HD), HS-SPME provide the advantages of a small amount of sample, time-saving, simplicity and cheapness.
authors.affiliation: a Department of Horticulture, College of Agriculture , Islamic Azad University , Maragheh , Iran.
authors.forename: Mohammad
authors.initials: M
authors.lastname: Nemati Kharajuo
authors.affiliation: b Faculty of Science, Department of Chemistry , University of Maragheh , Maragheh , Iran.
authors.forename: Marzieh
authors.initials: M
authors.lastname: Piryaei
authors.affiliation: a Department of Horticulture, College of Agriculture , Islamic Azad University , Maragheh , Iran.
authors.forename: Marzieh
authors.initials: M
authors.lastname: Babashpour Asl
authors.affiliation: b Faculty of Science, Department of Chemistry , University of Maragheh , Maragheh , Iran.
authors.forename: Mir Mahdi
authors.initials: MM
authors.lastname: Abolghasemi
mesh_terms: D000535:Aluminum / Q000737:chemistry*; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods; D032411:Lippia / Q000737:chemistry*; D058608:Nanopores; D052617:Solid Phase Microextraction / Q000379:methods*; D013696:Temperature; D013997:Time Factors; D055549:Volatile Organic Compounds / Q000032:analysis*
chemical_list: D055549:Volatile Organic Compounds; D000535:Aluminum
keywords: Lippia citriodora; Nanoporous aluminium; microextraction