title: Effect of prior deformation on microstructural development and Laves phase precipitation in high-chromium stainless steel.
abstract: This study investigated the influence of deformation on precipitation behaviour and microstructure change during annealing. Here, the prior deformation of high-chromium stainless steel was tensile deformation of 3%, 6% and 10%, and the specimens were then annealed at 700˚C for 10 h. The specimens were subsequently analyzed using backscattered electron image and electron backscattering diffraction measurements with SEM. Compared with the deformation microstructure, the grains revealed no preferred orientation. The precipitates of TiN and NbC were formed homogenously in the grain interior and at grain boundaries after annealing. Fine Laves phase precipitates were observed in grains and along subgrain boundaries as the deformation increased. Furthermore, the volume fraction of Laves phase increased, but the average particle diameter of precipitate was reduced as the deformation increased.
authors.affiliation: Department of Materials Science and Engineering, National Cheng-Kung University Road, Tainan 701, Taiwan.
authors.forename: Z-W
authors.initials: ZW
authors.lastname: Hsiao
authors.affiliation: China Steel Corporation, Kaohsiung, Taiwan.
authors.forename: D
authors.initials: D
authors.lastname: Chen
authors.affiliation: Department of Materials Science and Engineering, National Cheng-Kung University Road, Tainan 701, Taiwan.
authors.forename: J-C
authors.initials: JC
authors.lastname: Kuo
authors.affiliation: Department of Chemical and Materials Engineering, National University of Kaohsiung, Kaohsiung, Taiwan.
authors.forename: D-Y
authors.initials: DY
authors.lastname: Lin
keywords: Crofer 22 H; EBSD; Laves phase; strain-induced precipitates