title: Multi-Mycotoxin Analysis in Durum Wheat Pasta by  Liquid Chromatography Coupled to Quadrupole  Orbitrap Mass Spectrometry.
abstract: A simple and rapid multi-mycotoxin method for the determination of 17 mycotoxins  simultaneously  is  described  in  the  present  survey  on  durum  and  soft  wheat  pasta  samples.  Mycotoxins included in the study were those mainly reported in cereal samples: ochratoxin-A  (OTA), aflatoxin B1 (AFB1), zearalenone (ZON), deoxynivalenol (DON), 3-and 15-acetyl-deoxynivalenol  (3-AcDON and 15-AcDON), nivalenol (NIV), neosolaniol (NEO), fusarenon-X, (FUS-X), T-2 toxin  (T-2) and HT-2 toxin (HT-2), fumonisin B1 and B2 (FB1 and FB2), and four emerging mycotoxins:  three  enniatins  (ENA,  ENA1,  and  ENB),  and  beauvericin  (BEA).  Twenty-nine  samples  were  analyzed to provide an overview on mycotoxin presence: 27 samples of durum wheat pasta, and  two samples of baby food. Analytical results concluded that trichothecenes showed the highest  incidence, mainly DON, NIV, and HT-2 toxin, followed by ZON and ENB, while NEO, FUS-X, OTA,  AFB1, and FUM were not detected in any sample. The highest contents corresponded to ENB and  ranged from 91.15μg/kg to 710.90 μg/kg.
authors.affiliation: Laboratory of Food Chemistry and Toxicology, Faculty of Pharmacy, University of Valencia, Av. Vicent Andrés Estellés s/n, 46100 Burjassot, València, Spain. josefa.tolosa@uv.es.|Department of Pharmacy, Faculty of Pharmacy, University of Naples "Federico II", Via Domenico Montesano 49, 80131 Napoli, Italy. josefa.tolosa@uv.es.
authors.forename: Josefa
authors.initials: J
authors.lastname: Tolosa
authors.affiliation: Department of Pharmacy, Faculty of Pharmacy, University of Naples "Federico II", Via Domenico Montesano 49, 80131 Napoli, Italy. giulia.graziani@unina.it.
authors.forename: Giulia
authors.initials: G
authors.lastname: Graziani
authors.affiliation: Department of Pharmacy, Faculty of Pharmacy, University of Naples "Federico II", Via Domenico Montesano 49, 80131 Napoli, Italy. annagaspari@virgilio.it.
authors.forename: Anna
authors.initials: A
authors.lastname: Gaspari
authors.affiliation: Department of Pharmacy, Faculty of Pharmacy, University of Naples "Federico II", Via Domenico Montesano 49, 80131 Napoli, Italy. donato.chianese@gmail.com.
authors.forename: Donato
authors.initials: D
authors.lastname: Chianese
authors.affiliation: Laboratory of Food Chemistry and Toxicology, Faculty of Pharmacy, University of Valencia, Av. Vicent Andrés Estellés s/n, 46100 Burjassot, València, Spain. emilia.ferrer@uv.es.
authors.forename: Emilia
authors.initials: E
authors.lastname: Ferrer
authors.affiliation: Laboratory of Food Chemistry and Toxicology, Faculty of Pharmacy, University of Valencia, Av. Vicent Andrés Estellés s/n, 46100 Burjassot, València, Spain. jordi.manes@uv.es.
authors.forename: Jordi
authors.initials: J
authors.lastname: Mañes
authors.affiliation: Department of Pharmacy, Faculty of Pharmacy, University of Naples "Federico II", Via Domenico Montesano 49, 80131 Napoli, Italy. alberto.ritieni@unina.it.
authors.forename: Alberto
authors.initials: A
authors.lastname: Ritieni
mesh_terms: D004784:Environmental Monitoring; D005506:Food Contamination / Q000032:analysis*; D019648:Foods, Specialized / Q000032:analysis; D007558:Italy; D009183:Mycotoxins / Q000032:analysis*; D014908:Triticum
chemical_list: D009183:Mycotoxins
keywords: baby‐food;  HRMS‐orbitrap;  durum wheat pasta;  multi‐residual method